Properties of TEMPO-oxidized cellulose nanofiber by using aqueous counter collision

Le Van Hai; Lindong Zhai; Jung Woong Kim; Eun-sik Choi; Jaehwan Kim

doi:10.1117/12.2259841

17 April 2017 Properties of TEMPO-oxidized cellulose nanofiber by using aqueous counter collision

Le Van Hai, Lindong Zhai, Jung Woong Kim, Eun-sik Choi, Jaehwan Kim

Proceedings Volume 10167, Nanosensors, Biosensors, Info-Tech Sensors and 3D Systems 2017; 101670G (2017) https://doi.org/10.1117/12.2259841
Event: SPIE Smart Structures and Materials + Nondestructive Evaluation and Health Monitoring, 2017, Portland, Oregon, United States

Abstract

Cellulose nanofiber (CNF) isolation from different resources influences the characteristics of the CNF. There are two methods to isolate CNFs, chemical and physical methods. This paper deals with a 2,2,6,6-tetramethylpiperidine- 1-oxylradical (TEMPO-oxidation) chemical method and aqueous counter collision physical method to isolate CNFs. TEMPO-oxidized cellulose nanofiber was isolated using an aqueous counter collision method from two cellulose resource including Softwood bleached kraft pulp (SW) and Hardwood bleached kraft pulp (HW) resources. The CNFs properties were studied by atomic force microscopy, cross-polarize light and UV visible spectrometer. The width of the isolated CNFs is in the range of 15 nm to 20 nm and the length of cellulose nanofibers is around 1000 nm. The HW-CNF offers better transmittance than the SW-CNF. High transmittance of CNF films from both SWCNF and HW-CNF was observed. In addition, the birefringence of CNFs was observed under cross polarized light. The SW-CNF and HW-CNF films showed birefringence phenomenon. More clear iridescence color of HW-CNF sample than that of SW-CNF case.

Conference Presentation

Citation Download Citation

Le Van Hai, Lindong Zhai, Jung Woong Kim, Eun-sik Choi, and Jaehwan Kim "Properties of TEMPO-oxidized cellulose nanofiber by using aqueous counter collision", Proc. SPIE 10167, Nanosensors, Biosensors, Info-Tech Sensors and 3D Systems 2017, 101670G (17 April 2017); https://doi.org/10.1117/12.2259841

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