Open Access Paper
6 October 2003 Method to make accurate measurements of refractive index
Carlos Robledo-Sánchez, Nazario Bautista-Elivar
Author Affiliations +
Proceedings Volume 9663, Eighth International Topical Meeting on Education and Training in Optics and Photonics; 96632L (2003) https://doi.org/10.1117/12.2207471
Event: Eighth International Topical Meeting on Education and Training in Optics and Photonics, 2003, Tucson, Arizona, United States
Abstract
We propose in this work the use a diffraction grating to calculate the wavelength inside a transparent material of parallel plane faces, with the purpose of measuring the magnitude of their refractive index. The errors of this method and the precision are discussed.

1.

Introduction

One of the important parameters used in optics is the refractive index. There are different methods to measure the refractive index in the visible region. One of the techniques used to carry out these measurements uses the method of minimum deviation that suffers a ray of light when crossing a prism(1). Other common methods are based on the determination of the critical angle and in the Brewster angle(2). A method of determination of the refractive index using prisms was described recently by Hsiu(3). In the method of Hsiu, the incident beam is normal to the first surface of the prism the refraction is manifested only in the second surface. The relationship obtained under this configuration is n = sen(α + δ)/sen α, where α the angle of the prism and δ the deviation angle that suffers the beam in the second surface. The method of Hsiu can be used to determine refractive index of lens doing some modifications. Most of these methods are based on the application of the refraction law. The method that we propose in this paper considers the diffraction of the light.

2.

Theory

The diffraction grating is normally used for measuring wavelength through the grating equation

00092_psisdg9663_96632L_page_1_1.jpg

for the case when the incident plane wavefronts of light make an angle of 0° with the plane of the grating, m is order of interference. The zero-order principal maximum provides no information about the wavelength of the illumination. Information about the wavelength of the illuminating light can only be obtained by measuring the angular position of the higher-order principal maximum. We will employ this method for measuring wavelength inside of a optic glass. It is known that a wave inside a transparent material changes its space period in the form(4)

00092_psisdg9663_96632L_page_2_1.jpg

this result is used to measure n measuring the wavelength λ′ inside the material and using λ of a well-known source. Considering the Ec.(1) the separation dy of two diffraction orders is

00092_psisdg9663_96632L_page_2_2.jpg

where s is the distance from the grating to observation screen, a is the separation of slits. If the same experiment is realized inside a material with n index, then the wavelength change by

00092_psisdg9663_96632L_page_2_3.jpg

Finally using the Ec. (1) we can obtain n calculating λ/λ′; where λ is the wavelength in the vacuum of a well-known source, λ′ is the wavelength inside the material. Substituting the Ec. (4) and Ec. (5) into the Ec. (2) that n = λ/λ′ can be obtained by

00092_psisdg9663_96632L_page_2_4.jpg

where dy and dy′ are the separation of diffraction orders when the experiment is realized in the vacuum and inside a material, respectively.

2.

Experimental procedure

The experimental setup consist of a He-Ne laser of 3 mW and 632.8 nm and optical glass cube as material under test. The cube is mounted on a XY positioning stage platform. The parameter a of the diffraction grating used is 6.81 microns. The measurements of dy′ and dy′ was carry out with a CCD camera. The measurements was doing placing the diffraction grating close to the DA face of the cube see Fig.1, measuring the separation dy′ among -1 and +1 diffracted orders in the opposite face CD of the cube. Subsequently we measure dy among the same orders but now outside of the cube. The pattern of diffraction inside the cube is observed in the CB face and outside in the BF face, see Fig. 1.

Fig. 1.

Experimental setup to measuring the refraction index of a optical glass cube using diffraction.

00092_psisdg9663_96632L_page_3_1.jpg

To observe the diffraction grating we put a diffuser sheet in the CB face of the cube. To observe the diffraction pattern inside and outside of the cube this was translated laterally in the Y direction. The measurements was realize with a CCD camera with a zoom lens. The Fig. 2 show the diffraction patterns obtained.

Fig. 2.

Diffraction patterns.

00092_psisdg9663_96632L_page_4_1.jpg

Results

Using the images of Fig. 2 we obtained the value of dy' and dy of 190.1 and 289 pixels, respectively. Giving the magnitude of 1.521 for the refractive index. The value specified of n is 1.52504 for the He-Ne laser. Our result obtained has a precision of 0.2 %.

Conclusions

We used a diffraction experiment to calculate the refractive index of a glass cube. This method is simple and has good precision. This experiment can be use to show in the classroom in an elementary optics course the effect of how the wavelength change inside the materials. The method gives as an alternative technique of easy implementation in ours optics laboratories.

One of authors N. Bautista-Elivar thanks the support granted by CONACyT.

References

(1) 

R.S. Longhurst, “Geometrical and physical optics,” 72 –73 Longmans, Green, New York london (1962). Google Scholar

(2) 

C. Harvey Palmer, “Optics, experiments and demotrations,” the Johns-Hopkins Press, Baltimore (1962). Google Scholar

(3) 

H.Hsiu, “Accurate measurement of refractive index,” Eng. Lab. Notes in opt. \& phot. News s-4, (1993). Google Scholar

(4) 

P. Hariharan, “Optical interferometry,” Academic Press, Inc. (1985). Google Scholar
© (2003) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.
Carlos Robledo-Sánchez and Nazario Bautista-Elivar "Method to make accurate measurements of refractive index", Proc. SPIE 9663, Eighth International Topical Meeting on Education and Training in Optics and Photonics, 96632L (6 October 2003); https://doi.org/10.1117/12.2207471
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KEYWORDS
Refractive index

Diffraction

Diffraction gratings

Glasses

Prisms

Error analysis

Helium neon lasers

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