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The growth of Li1+xMn2O4 via detonation reaction was investigated with respect to the presence of energetic precursors,
such as the metallic nitrates and the degree of confinement of the explosive charge. The detonation products were
characterized by scanning electron microscopy. Powder X-ray diffraction and transmission electron microscopy were
used to characterize the products. Li1+xMn2O4 with 1~2μm spherical morphology and more uniform secondary particles,
but with smaller primary particles of diameters from 20 to 60 nm and a variety of morphologies were found. The oxides
produced by this cheap method affirmed the validity of detonation synthesis of nano-size powders.
Xinghua Xie,Jing Zhu,Huisheng Zhou, andShilong Yan
"Nanometer functional materials from explosives", Proc. SPIE 7493, Second International Conference on Smart Materials and Nanotechnology in Engineering, 74931P (20 October 2009); https://doi.org/10.1117/12.835722
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Xinghua Xie, Jing Zhu, Huisheng Zhou, Shilong Yan, "Nanometer functional materials from explosives," Proc. SPIE 7493, Second International Conference on Smart Materials and Nanotechnology in Engineering, 74931P (20 October 2009); https://doi.org/10.1117/12.835722